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A method for the solvent-free photocatalytic conversion of solid and liquid substrates was developed, using a novel rod mill apparatus. In this setup, thin liquid films are realized which is crucial for an effective photocatalytic conversion due to the low penetration depth of light in heterogeneous systems.

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These K-OMS-2 materials show improved catalytic activity for the oxidation of alcohols compared with the conventional K-OMS-2 materials, which may be due to their higher surface areas and novel ...

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Oxidation of Alcohols. Reaction type: Oxidation-Reduction. Summary. Common reagents: The outcome of oxidation reactions of alcohols depends on the substituents on the carbinol carbon. In order for each oxidation step to occur, there must be H on the carbinol carbon. Primary alcohols can be oxidised to aldehydes or further to carboxylic acids.

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Nov 01, 2017· Aerobic oxidation of alcohols. A mixture of K 2 CO 3 (1 mmol) and the catalyst (10 mg) in toluene (5 mL) was prepared in a two necked flask. The flask was evacuated and refilled with pure oxygen. To this solution, the alcohol (1 mmol, in 1 mL toluene) was injected and the resulting mixture was stirred at 80 °C under an oxygen atmosphere.

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Oct 27, 2016· In mechanochemistry, reactions are performed by grinding the reaction mixture in ball mills, such as the vibrational ball mill or the planetary ball mill, or with a pestle and mortar. In preliminary studies, we tested a vibrational ball mill for photocatalytic oxidations with riboflavin tetraacetate, using a transparent milling chamber.

In 2015, Mal et al. reported the first example of a very interesting solvent free ball-milling oxidation of activated primary alcohols to aldehyde using NBS (1.5 equiv) or oxone (0.6 equiv) as co-oxidising agents. This paper has laid the foundation for further studies on this topic.

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Nov 23, 2011· In the presence of a manganese oxide based octahedral molecular sieve (OMS‐2), a range of primary amides could be synthesized directly from primary alcohols and ammonia (see scheme). The observed catalysis was heterogeneous, and the recovered catalyst could be reused many times without an appreciable loss of its catalytic performance.

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Mixed‐valent manganese octahedral molecular sieves K‐OMS‐2 and H‐K‐OMS‐2 are used to oxidize a wide range of alcohols with 100 % selectivity and 90–100 % conversion in most cases. The reaction (see scheme) is aerobic, catalytic, mild, efficient, stable, inexpensive, selective, and …

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